HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanamine, hydrochloride (1:1) → HCID 66925152, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanamine, hydrochloride (1:1) | HCID 11637 | — |
| Reactant | Sodium cyanoborohydride | HCID 5003444 | — |
| Reactant | HCID 86620745 | HCID 86620745 | — |
| Product | HCID 66925152 | HCID 66925152 | 65.5% |
Reaction Steps
Using 1-[(3-chlorophenyl)sulfonyl]-2-methyl-5-phenyl-1H-pyrrole-3-carbaldehyde (171 mg), methylammonium chloride (311 mg) and sodium cyanoborohydride (103 mg), a procedure as in Example 4 was performed to give the title compound as a colorless oil (yield 64 mg, 34%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08048909B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-e90679bd31a74292b62c8c7b1de46f0a |
| Source note | uspto-grants-2011_11 |