HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 66924687, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | Monomethylamine methanol | HCID 57454252 | — |
| Reactant | HCID 86620779 | HCID 86620779 | — |
| Product | HCID 66924687 | HCID 66924687 | 24% |
Reaction Steps
Using 2-chloro-4-[(4-formyl-2-phenyl-1H-pyrrol-1-yl)sulfonyl]benzonitrile (248 mg), 40% methylamine methanol solution (1.4 mL) and sodium borohydride (28.9 mg), a procedure as in Example 9 was performed to give the title compound as white crystals (yield 67.8 mg, 24%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08048909B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-abc622816934403e8ab644cc0dea0cbf |
| Source note | uspto-grants-2011_11 |