HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen chloride-ethyl acetate → HCID 66925289, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Reactant | HCID 86620792 | HCID 86620792 | — |
| Product | HCID 66925289 | HCID 66925289 | 14% |
Reaction Steps
Using tert-butyl ({1-[(4-cyano-3-fluorophenyl)sulfonyl]-5-phenyl-1H-pyrrol-3-yl}methyl)carbamate (54.7 mg) and 4 mol/L hydrogen chloride-ethyl acetate solution (4 mL), a procedure as in Example 30 was performed to give the title compound as a white solid (yield 6.9 mg, 14%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08048909B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-af40db080fdf41e1893e06bf2369a22f |
| Source note | uspto-grants-2011_11 |