Acrylic Acid → HCID 22481283, compound
Reaction equation
[C:1]([O:5][CH2:6][CH2:7][CH2:8][CH3:9])(=[O:4])[CH:2]=[CH2:3].[C:10]([OH:14])(=[O:13])[CH:11]=[CH2:12]>>[C:1]([O:5][CH2:6][CH2:7][CH2:8][CH3:9])(=[O:4])[CH:2]=[CH2:3].[C:10]([OH:14])(=[O:13])[CH:11]=[CH2:12]Participants
Procedure
A synthesis was conducted by the same procedure as in the resin 1 except that n-butyl acrylate (nBA) and acrylic acid (AA) were used as monomers, thereby obtaining an nBA-AA type resin 3. The resin 3 was neutralized with an aqueous solution of potassium hydroxide to obtain an aqueous solution having a solid content concentration of 20% by mass. Incidentally, the resin 3 was in a state dissolved in the aqueous solution, and so the 50% cumulative volume average particle size (D50) of the resin 3 could not be measured. The weight average molecular weight of the resin 3 in terms of polystyrene was 9,000. The glass transition temperature of the resin 3 was 20° C. The acid value of the resin 3 as measured by a neutralization titration method was 260 mg KOH/g.
Sources & evidence
- ORD record
- ord-b494720ffb4641b78efe582ec721a73e
- Source dataset
- uspto-grants-2011_11
- Patent number
- US08052271B2
Reaction notes
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