1,2-Dichloroethane → HCID 11360779, compound

Participants

Reaction Steps

To a solution of 2,3-diamino toluene (45 mg, 0.368 mmol) in DCE (2 mL) was slowly added 1c (50 mg, 0.176 mmol). The reaction was stirred 18 h at rt and concentrated. The crude mixture containing 1d and 1d′ was used in the next step without further purification. [M+H]+=407.4.

Provenance & Evidence