HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Tert-butylbenzene-1,2-diamine → HCID 11362786, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Tert-butylbenzene-1,2-diamine | HCID 432708 | — |
| Reactant | HCID 59857516 | HCID 59857516 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 11362786 | HCID 11362786 | — |
Reaction Steps
To a solution of 4-(tert-butyl)-1,2-diaminobenzene (20 mg, 0.12 mmol) in DCE (1 mL) was slowly added 2c (19 mg, 0.06 mmol). The reaction was stirred 18 h at rt and concentrated. The crude mixture containing 2d and 2d′ was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08053450B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-73980c66a9184a70a27842c939169a66 |
| Source note | uspto-grants-2011_11 |