HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Tert-butylbenzene-1,2-diamine → HCID 11441710, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Tert-butylbenzene-1,2-diamine | HCID 432708 | — |
| Reactant | HCID 21487087 | HCID 21487087 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 11441710 | HCID 11441710 | — |
Reaction Steps
To a solution of 4-(tert-butyl)-1,2-diaminobenzene (20 mg, 0.12 mmol) in DCE (1 mL) was slowly added 3c (19 mg, 0.06 mmol). The reaction was stirred 18 h at rt and concentrated. The crude mixture containing 3d and 3d′ was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08053450B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-5fc5bb685c7147248ab136c5e159944b |
| Source note | uspto-grants-2011_11 |