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HRID555480

反应详情

EQUATION

反应方程式

HRID 555480 的结构方程式

REACTANTS

反应物

3
结构：CN(C)c1ccc(C=O)c2ccccc12
HCID608052

4-Dimethylamino-1-naphthaldehyde

C13H13NO

结构：COc1cc(N)c(C(N)=O)c(OC)c1
HCID20349016

2-Amino-4,6-dimethoxybenzamide

C9H12N2O3

结构：COc1cc(OC)c2c(=O)[nH]c(-c3ccccn3)nc2c1
HCID136037998

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc(OC)c2c(=O)[nH]c(-c3ccc(N(C)C)c4ccccc34)nc2c1
HCID136037975

未命名化合物

收率 26%

PROCEDURE

实验过程

2-(4-(Dimethylamino)naphthalen-1-yl)-5,7-dimethoxyquinazolin-4(3H)-one was synthesized from 2-amino-4,6-dimethoxybenzamide and 4-dimethylamino-1-naphthaldehyde, using the method described for 5,7-dimethoxy-2-(pyridin-2-yl)quinazolin-4(3H)-one. 2-(4-(Dimethylamino)naphthalen-1-yl)-5,7-dimethoxyquinazolin-4(3H)-one (75 mg, 26%) was isolated as a yellow solid. Selected data: MS (m/z): 376.07; MP 269-271° C.