huagongshe.com
HRID555490

反应详情

EQUATION

反应方程式

HRID 555490 的结构方程式

REACTANTS

反应物

3
结构：NC(=O)c1ccccc1N
HCID6942

2-Aminobenzamide

C7H8N2O

结构：O=Cc1ccc(N(CCO)CCO)cc1
HCID12824965

4-[Bis(2-hydroxyethyl)amino]benzaldehyde

C11H15NO3

结构：COc1cc(OC)c2c(=O)[nH]c(-c3ccccn3)nc2c1
HCID136037998

未命名化合物

PRODUCTS

生成物

1
结构：O=c1[nH]c(-c2ccc(N(CCO)CCO)cc2)nc2ccccc12
HCID136038001

未命名化合物

收率 42%

PROCEDURE

实验过程

2-(4-(Bis(2-hydroxyethyl)amino)phenyl)quinazolin-4(3H)-one was synthesized from anthranilamide and 4-[bis-(2-hydroxy-ethyl)-amino]-benzaldehyde, using the method described for 5,7-dimethoxy-2-(pyridin-2-yl)quinazolin-4(3H)-one. 2-(4-(Bis(2-hydroxyethyl)amino)phenyl)quinazolin-4(3H)-one (150 mg, 42%) was isolated as a brown solid. Selected data: MS (m/z): 326.03; MP 228-230° C.