HuagongsheHuagongshe Chemistry Print Report · For research reference only
(Phenylmethyl)hydrazine → HCID 46193502, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (Phenylmethyl)hydrazine | HCID 11157 | — |
| Reactant | p-Methoxycarbonylphenyl 2-selenophenyl ketone | HCID 46193254 | — |
| Reactant | HCID 46193500 | HCID 46193500 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 46193502 | HCID 46193502 | — |
Reaction Steps
Compound 63 (5.86 g, 0.02 mole), benzylhydrazine 50 (4.88 g, 0.04 mole) and glacial acetic acid (1.5 ml) were allowed to react as in the preparation of compound 55 to afford compound 67. Yield: 2.49 g (31.4%); white crystals; mp 150-153° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08053459B1 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-4156d3071a3343a18d49e066173fd7b5 |
| Source note | uspto-grants-2011_11 |