HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylhydrazine → HCID 54588370, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylhydrazine | HCID 7516 | — |
| Reactant | HCID 46193500 | HCID 46193500 | — |
| Reactant | HCID 86761434 | HCID 86761434 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 54588370 | HCID 54588370 | — |
Reaction Steps
Compound 73 (3.8 g, 0.013 mole), phenylhydrazine 8 (5.0 g, 0.046 mole) and glacial acetic acid (1.5 ml) were allowed to react as in the preparation of compound 55 to afford compound 78. Yield: 0.62 g (12.8%); white needle crystals; mp 167-169° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08053459B1 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-56d2a72d352940eb9c1b3c0790fe7a00 |
| Source note | uspto-grants-2011_11 |