HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyethanol → HCID 63083697, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyethanol | HCID 8019 | — |
| Reactant | 4-Chloro-2-fluorobenzonitrile | HCID 93655 | — |
| Product | HCID 63083697 | HCID 63083697 | — |
Reaction Steps
The title compound is synthesized by coupling followed by reduction of 4-chloro-2-fluoro-benzonitrile and 2-methoxy-ethanol analogously to the preparation of Intermediate 98.1 as a colorless solid; ES-MS: M+=216.1; HPLC: AtRet=2.51 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08053457B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-de468276ba744d84ad9e07fa42c4b6a1 |
| Source note | uspto-grants-2011_11 |