HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxy-1-propanol → HCID 63081121, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxy-1-propanol | HCID 74116 | — |
| Reactant | 4-Chloro-2-fluorobenzonitrile | HCID 93655 | — |
| Product | HCID 63081121 | HCID 63081121 | — |
Reaction Steps
The title compound is synthesized by coupling followed by reduction of 4-chloro-2-fluoro-benzonitrile and 3-methoxy-propanol analogously to the preparation of Intermediate 98.1 as a colorless solid; ES-MS: M+=230.1; HPLC: AtRet=2.81 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08053457B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-bd3837aa46f944a6a5b26c260025d738 |
| Source note | uspto-grants-2011_11 |