HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Propanediol → HCID 63082662, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Propanediol | HCID 10442 | — |
| Reactant | 4-Chloro-2-fluorobenzonitrile | HCID 93655 | — |
| Product | HCID 63082662 | HCID 63082662 | — |
Reaction Steps
The title compound is synthesized by coupling followed by reduction of 4-chloro-2-fluoro-benzonitrile and 1,3-propane-diol analogously to the preparation of Intermediate 113.1 as a colorless solid; ES-MS: M+=216.1; HPLC: AtRet=2.23 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08053457B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-f16fac01b4504fb3a3d9837a2bad6463 |
| Source note | uspto-grants-2011_11 |