N,N-Dimethylethylenediamine → HCID 63082312, compound

Participants

Reaction Steps

The title compound is synthesized by coupling followed by reduction of 4-chloro-2-fluoro-benzonitrile and 2-dimethylamino-ethylamine analogously to the preparation of Intermediate 113.1 as a colorless oil; 1HNMR (CDCl3) δ 9.20 (bs, 1H), 7.18-7.10 (m, 2H), 6.95 (d, 1H), 4.60 (s, 2H), 3.80 (s, 2H), 3.25-3.05 (m, 4H), 2.25 (s, 6H); HPLC: AtRet=1.26 min.

Provenance & Evidence