Bromoacetonitrile → HCID 61951591, compound

Participants

Reaction Steps

The title compound is synthesized by coupling of 1-Cyclohexylmethyl-piperazine piperazine (commercially available from Fluorochem Ltd) and bromoacetonitrile analogously to the preparation of Intermediate 149.2 as a colorless oil; ES-MS: M+=222.2: 1HNMR(DMSO-d6) 3.65 (s, 2H), 2.45-2.20 (m, 8H), 2.00 (d, 2H), 1.70-1.55 (m, 5H), 1.50-1.40 (m, 1H), 1.20-1.05 (m, 3H), 0.85-0.70 (m, 2H).

Provenance & Evidence