HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromoacetonitrile → HCID 86641788, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromoacetonitrile | HCID 11534 | — |
| Reactant | 4-Morpholinopiperidine | HCID 795724 | — |
| Product | HCID 86641788 | HCID 86641788 | — |
Reaction Steps
The title compound is synthesized by coupling of 4-Piperidin-4-yl-morpholine (commercially available from CHESS GmbH) and bromoacetonitrile analogously to the preparation of Intermediate 149.2 as a colorless oil; ES-MS: M+=210.1: 1HNMR(DMSO-d6) 3.65 (s, 2H), 3.55 (t, 4H), 2.80-2.75 (m, 2H), 2.40 (t, 4H), 2.15-2.00 (m, 3H), 1.80-1.70 (m, 2H), 1.40-1.30 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08053457B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-3096b66636b5464b9b6db85fb81da4ab |
| Source note | uspto-grants-2011_11 |