HRID555750

反应详情

EQUATION

反应方程式

HRID 555750 的结构方程式

PROCEDURE

实验过程

The title compound is synthesized by coupling of 1-Pyridin-4-ylmethyl-piperazine (commercially available from ABCR GmbH) and bromoacetonitrile analogously to the preparation of Intermediate 149.2 as a colorless oil; ES-MS: M+=217.2: 1HNMR(CDCl3) 8.55 (d, 2H), 7.25 (d, 2H), 3.50 (s, 4H), 2.70-2.40 (m, 8H).

WORKUP

后处理

  1. customanalogously to the preparation of Intermediate 149.2 as a colorless oil