HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromoacetonitrile → HCID 43430780, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromoacetonitrile | HCID 11534 | — |
| Reactant | N,N-Dimethylpiperidin-4-amine | HCID 417391 | — |
| Product | HCID 43430780 | HCID 43430780 | — |
Reaction Steps
The title compound is synthesized by coupling of Dimethyl-piperidin-4-yl-amine and bromoacetonitrile analogously to the preparation of Intermediate 149.2 as a colorless oil; ES-MS: M+=168.1: 1HNMR(DMSO-d6) 3.65 (s, 2H), 2.80-2.75 (m, 2H), 2.15-2.05 (m, 8H, including a singlet at 2.10), 2.00-1.95 (m, 1H), 1.75-1.65 (m, 2H), 1.40-1.30 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08053457B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-6d3d3d894d27443d8a39d5041de8edb1 |
| Source note | uspto-grants-2011_11 |