HRID555755

反应详情

EQUATION

反应方程式

HRID 555755 的结构方程式

PROCEDURE

实验过程

The title compound is synthesized by coupling of Diethyl-piperidin-4-yl-amine (commercially available from CHESS GmbH) and bromoacetonitrile analogously to the preparation of Intermediate 149.2 as a colorless oil; ES-MS: M+=196.2: 1HNMR(DMSO-d6) 3.65 (s, 2H), 2.80-2.75 (m, 2H), 2.45-2.30 (m, 5H), 2.15-2.05 (m, 2H), 1.70-1.60 (m, 2H), 1.45-1.35 (m, 2H), 0.95 (t, 6H).

WORKUP

后处理

  1. customanalogously to the preparation of Intermediate 149.2 as a colorless oil