HRID555756

反应详情

EQUATION

反应方程式

HRID 555756 的结构方程式

PROCEDURE

实验过程

The title compound is synthesized by coupling of 1-Adamantyl-piperazine (commercially available from CHESS GmbH) and bromoacetonitrile analogously to the preparation of Intermediate 149.2 as a colorless oil; ES-MS: M+=260.3: 1HNMR(DMSO-d6) 3.65 (s, 2H), 2.60-2.50 (m, 4H), 2.45-2.40 (m, 4H), 2.00 (bs, 3H), 1.60-1.50 (m, 12H).

WORKUP

后处理

  1. customanalogously to the preparation of Intermediate 149.2 as a colorless oil