HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Anisoyl chloride → HCID 178490480, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Anisoyl chloride | HCID 74374 | — |
| Reactant | HCID 178507674 | HCID 178507674 | — |
| Product | HCID 178490480 | HCID 178490480 | 9% |
Reaction Steps
The title compound was prepared essentially according to the method of Example 4, but using 5-Chloro-2-(1H-tetrazol-5-yl)aniline (1.0 mmol) and 3-methoxybenzoyl chloride to afford the desired product (29.1 mg, 9%). 1H NMR (400 MHz, d6-DMSO): δ 10.81 (s, 1H), 8.75 (s, 1H), 8.06 (s, 1H), 7.60 (m, 3H), 7.25 (s, 1H), 3.89 (s, 3H). MS (EI) for C15H12ClN5O2: 329.7 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08053454B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-3a018cc7b1c94cad8933619577ed699f |
| Source note | uspto-grants-2011_11 |