HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 66992094, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 66991737 | HCID 66991737 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 66992094 | HCID 66992094 | 100.8% |
Reaction Steps
3-[2-methoxy-4-(3-oxo-3-phenyl-propenyl)-phenyl]-acrylic acid tert-butyl ester (635 mg, 1.74 mmol) was dissolved in DCM (12 ml) and TFA (3 ml) was added to the resulting solution. After stirring for 2 h at room temperature the solvent was removed under vacuo giving 541 mg of 3-[2-methoxy-4-(3-oxo-3-phenyl-propenyl)-phenyl]-acrylic acid as yellow powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08058273B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-a4e30743e99e4a598e5ee955199a6d9e |
| Source note | uspto-grants-2011_11 |