HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 59639578, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Trimethylaluminum | HCID 16682925 | — |
| Reactant | HCID 59639612 | HCID 59639612 | — |
| Product | HCID 59639578 | HCID 59639578 | 54.5% |
Reaction Steps
Following the general procedure outlined in Example 193, dimethylamine (1.1 mL, 2.2 mmol), trimethylaluminum (1.1 mL, 2.2 mmol) and the product of Example 190 (100 mg, 0.22 mmol) were reacted to give the desired product 56 mg (54%). LC-MS: 468.2 (MH+, m/z), 2.00 (Rt, min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08058282B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-88e0926b81b14dcd90a81d106177ff54 |
| Source note | uspto-grants-2011_11 |