HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 66765778, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Pivaloyl chloride | HCID 62493 | — |
| Reactant | HCID 66765802 | HCID 66765802 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 66765778 | HCID 66765778 | — |
Reaction Steps
To a solution of 1-deoxy-1-(2,4-dimethoxyphenyl)-β-D-glucopyranose (0.47 g) in pyridine (10 mL) was added pivaloyl chloride (1.1 g) at room temperature, and the mixture was stirred at room temperature overnight. The reaction mixture was poured into water, and the mixture was extracted with diethyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08058245B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-3a1d304941af4e2099980beb59e46fa0 |
| Source note | uspto-grants-2011_11 |