HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Thiophenecarboxaldehyde → HCID 11639091, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Thiophenecarboxaldehyde | HCID 68135 | — |
| Reactant | Acetic acid, 2,2'-[methylenebis(sulfonyl)]bis- | HCID 2252641 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 11639091 | HCID 11639091 | 55% |
Reaction Steps
A solution of thiophene-3-carbaldehyde (2 mmol) and carboxymethane-sulfonylmethanesulfonyl-acetic acid (1 mmol) in acetic acid (10 mL) was subjected to General Procedure 1, to yield the title compound in 55% yield. m.p. 150-152° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08058313B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-6b151e9dedaa4212a1ed0f49055f27e6 |
| Source note | uspto-grants-2011_11 |