HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzaldehyde → HCID 11653873, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzaldehyde | HCID 68023 | — |
| Reactant | Acetic acid, 2,2'-[methylenebis(sulfonyl)]bis- | HCID 2252641 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 11653873 | HCID 11653873 | 74% |
Reaction Steps
A solution of 4-fluorobenzaldehyde (2 mmol) and carboxymethane-sulfonylmethanesulfonyl-acetic acid (1 mmol) in acetic acid (10 mL) was subjected to General Procedure 1, to yield the title compound in 74% yield. m.p. 183-185° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08058313B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-23ea146504ed4137b523b4d16b5d3bb6 |
| Source note | uspto-grants-2011_11 |