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HRID557107

反应详情

EQUATION

反应方程式

HRID 557107 的结构方程式

REACTANTS

反应物

2
结构：COc1cc(O)cc(OC)c1C=O
HCID529894

4-Hydroxy-2,6-dimethoxybenzaldehyde

C9H10O4

结构：O=C(O)CS(=O)(=O)CS(=O)(=O)CC(=O)O
HCID2252641

Acetic acid, 2,2'-[methylenebis(sulfonyl)]bis-

C5H8O8S2

PRODUCTS

生成物

1
结构：COc1cc(O)cc(OC)c1/C=C/S(=O)(=O)CS(=O)(=O)/C=C/c1c(OC)cc(O)cc1OC
HCID11620311

未命名化合物

收率 62%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)O
溶剂HCID176

Acetic Acid

C2H4O2

PROCEDURE

实验过程

A solution of 4-hydroxy-2,6-dimethoxybenzaldehyde (2 mmol) and carboxymethane-sulfonylmethanesulfonyl-acetic acid (1 mmol) in acetic acid (10 mL) was subjected to General Procedure 1, to yield the title compound in 62% yield. m.p. 148-150° C.