HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isovanillin → HCID 86761436, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isovanillin | HCID 12127 | — |
| Reactant | Acetic acid, 2,2'-[methylenebis(sulfonyl)]bis- | HCID 2252641 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 86761436 | HCID 86761436 | 62% |
Reaction Steps
A solution of 3-hydroxy-4-methoxybenzaldehyde (2 mmol) and carboxymethane-sulfonylmethanesulfonyl-acetic acid (1 mmol) in acetic acid (10 mL) was subjected to General Procedure 1, to yield the title compound in 62% yield. m.p. 148-150° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08058313B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-bffc1ddb31e34525977172f74181c0f2 |
| Source note | uspto-grants-2011_11 |