HRID557135

反应详情

EQUATION

反应方程式

HRID 557135 的结构方程式

PROCEDURE

实验过程

1.00 g (3.54 mmol) 6-Methoxy-1-methyl-2-phenyl-1H-quinazolin-4-thione was slowly added to 5 ml (80 mmol) methyl iodide at 0° C. and stirred for 1 h at room temperature. The solution was filtrated and the residue washed with ethyl ether and dichloromethane.

WORKUP

后处理

  1. filtrationThe solution was filtrated
  2. washthe residue washed with ethyl ether and dichloromethane