HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 6-Methoxy-1-methyl-4-methylsulfanyl-2-phenyl-quinazolin-1-ium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 6-Methoxy-1-methyl-2-phenyl-1H-quinazolin-4-thione | HCID 86635531 | — |
| Product | 6-Methoxy-1-methyl-4-methylsulfanyl-2-phenyl-quinazolin-1-ium iodide | HCID 66991512 | — |
Reaction Steps
1.00 g (3.54 mmol) 6-Methoxy-1-methyl-2-phenyl-1H-quinazolin-4-thione was slowly added to 5 ml (80 mmol) methyl iodide at 0° C. and stirred for 1 h at room temperature. The solution was filtrated and the residue washed with ethyl ether and dichloromethane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08058431B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-787b722ca06a4837ae8704090947c732 |
| Source note | uspto-grants-2011_11 |