Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 5-Fluoro-2,3-dimethyl-benzothiazol-3-ium iodide | HCID 66990784 | — |
| Reactant | 6-Methoxy-1-methyl-4-methylsulfanyl-2-phenyl-quinazolin-1-ium iodide | HCID 66991512 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178487132 | HCID 178487132 | — |
Reaction Steps
600 mg (1.41 mmol) 6-Methoxy-1-methyl-4-methylsulfanyl-2-phenyl-quinazolin-1-ium iodide and 436 mg (1.41 mmol) 5-fluoro-2,3-dimethyl-benzothiazol-3-ium iodide were dissolved in 3.0 ml dimethylformamide and 571 mg (0.79 ml, 5.64 mmol) triethylamine were added. The solution was stirred for 1 h at 80° C., filtrated and the residue was washed with water and methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08058431B2 |
|---|
| Source dataset | uspto-grants-2011_11 |
|---|
| ORD ID | ord-34effdcaad544c3888d53f004b9d8346 |
|---|
| Source note | uspto-grants-2011_11 |
|---|
