Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2,3-Dimethylbenzo[d]thiazol-3-ium iodide | HCID 459121 | — |
| Reactant | 1-Methyl-4-methylsulfanyl-2-phenyl-thieno(3,2-d)pyrimidin-1-ium iodide | HCID 66991072 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178479927 | HCID 178479927 | — |
Reaction Steps
200 mg (0.50 mmol) 1-Methyl-4-methylsulfanyl-2-phenyl-thieno(3,2-d)pyrimidin-1-ium iodide and 145 mg (0.50 mmol) 2,3-dimethyl-benzothiazol-3-ium iodide were dissolved in 2.0 ml dimethylformamide and 202 mg (0.28 ml, 2.00 mmol) triethylamine were added. The green solution was stirred for 1 h at 80° C., filtrated and the residue was washed with methanol. The crude product was purified further by HPLC.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08058431B2 |
|---|
| Source dataset | uspto-grants-2011_11 |
|---|
| ORD ID | ord-0b7bf2fe6bb64c30b153690c4d80d56b |
|---|
| Source note | uspto-grants-2011_11 |
|---|
