反应详情

温度

80 °C

200 mg (0.50 mmol) 1-Methyl-4-methylsulfanyl-2-phenyl-thieno(3,2-d)pyrimidin-1-ium iodide and 145 mg (0.50 mmol) 2,3-dimethyl-benzothiazol-3-ium iodide were dissolved in 2.0 ml dimethylformamide and 202 mg (0.28 ml, 2.00 mmol) triethylamine were added. The green solution was stirred for 1 h at 80° C., filtrated and the residue was washed with methanol. The crude product was purified further by HPLC.

1. filtrationfiltrated
2. washthe residue was washed with methanol
3. customThe crude product was purified further by HPLC