HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → 2,3-Dimethoxy-6-nitrobenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | 2,3-Dimethoxybenzaldehyde | HCID 66581 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2,3-Dimethoxy-6-nitrobenzaldehyde | HCID 7172127 | — |
Reaction Steps
50.0 g (301 mmol) 2,3-Dimethoxy-benzaldehyd (Aldrich) were slowly added to nitric acid at 0° C. The reaction mixture was stirred for 5 minutes, diluted with water until no further precipitate was obtained. After filtration the residue was washed with methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08058431B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-c527207b313145dc8119198982e0cd7d |
| Source note | uspto-grants-2011_11 |