HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylenediamine → N~1~-(Pyridin-2-yl)ethane-1,2-diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | 2-Fluoropyridine | HCID 9746 | — |
| Product | N~1~-(Pyridin-2-yl)ethane-1,2-diamine | HCID 410428 | — |
Reaction Steps
Ethylenediamine (6 g, 0.1 mol) and 2-fluoropyridine (10 g, 0.1 mol) were heated neat at 120° C. overnight. The reaction was cooled and the residue was used in next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08058445B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-034ce77ba6404c0893cbfef2c3b075fa |
| Source note | uspto-grants-2011_11 |