HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 11609792, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 66661949 | HCID 66661949 | — |
| Catalyst | Pd barium sulfate | HCID 16218511 | — |
| Product | HCID 11609792 | HCID 11609792 | — |
Reaction Steps
To a solution of 1-{[1-(4-chlorophenyl)cyclopropyl]carbonyl}-3-(2-methylphenyl)-2,5-dihydro-1H-pyrrole (5 mg, 0.00001 mol) in methanol (1 mL, 0.02 mol) was added Pd/BaSO4 (reduced) and the mixture was stirred under an atmosphere of hydrogen at rt for 1 h. The crude product was purified using prep-HPLC. LCMS: m/z 340.4 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08058288B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-88a5dc09997c4f908793bc6858a38a3d |
| Source note | uspto-grants-2011_11 |