Hydrochloric Acid → HCID 66999864, compound

Participants

Reaction Steps

To a solution of 5-(2-(2-t-butoxycarbonylaminopyridin-4-yl) methylthiopyridin-3-yl)-N-phenyl-1,3,4-oxadiazol-2-amine (140 mg, 0.30 mmol; Compound 1-(7)) in dioxane (1.0 mL) was added a 4M dioxane solution of hydrogen chloride (1.0 mL, 4.0 mmol) at room temperature and then the mixture was stirred over night. The precipitated solid was filtered off to give 130 mg (quantitative) of the titled compound as a colorless solid.

Provenance & Evidence