m-Bromobenzenesulphonyl chloride → HCID 8469449, compound

HRID 558505Notes

Reaction equation

HRID 558505 reaction equation
[Br:1][C:2]1[CH:3]=[C:4]([S:8](Cl)(=[O:10])=[O:9])[CH:5]=[CH:6][CH:7]=1.[NH2:12][CH2:13][CH2:14][N:15]1[CH2:20][CH2:19][O:18][CH2:17][CH2:16]1>>[Br:1][C:2]1[CH:3]=[C:4]([S:8]([NH:12][CH2:13][CH2:14][N:15]2[CH2:20][CH2:19][O:18][CH2:17][CH2:16]2)(=[O:10])=[O:9])[CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 17943m-Bromobenzenesulphonyl chlorideHCID 4082852-Morpholinoethylamine

Product 1

HCID 8469449HCID 8469449, compoundYield 93%

Procedure

Prepared by general procedure III from 3-Bromobenzenesulfonyl chloride (5.0 g, 20 mmol) and 4-(2-Aminoethyl)-morpholine (2.80 mL, 22 mmol) to give the title compound (6.34 g, 93%) as a white solid. MS (ISN) 347.1 [(M−H)−], 349.3 [(M+2−H)−].

Sources & evidence

ORD record
ord-ac26159e2d0f402b81be736a0c4e288f
Source dataset
uspto-grants-2011_11
Patent number
US08063048B2

Reaction notes

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