p-Bromobenzenesulfonyl chloride → HCID 4378537, compound

HRID 558512Notes

Reaction equation

HRID 558512 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([S:8](Cl)(=[O:10])=[O:9])=[CH:4][CH:3]=1.[CH3:12][O:13][CH2:14][CH2:15][NH2:16]>>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([NH:16][CH2:15][CH2:14][O:13][CH3:12])(=[O:10])=[O:9])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 7396p-Bromobenzenesulfonyl chlorideHCID 80182-Methoxyethylamine

Product 1

HCID 4378537HCID 4378537, compoundYield 95%

Procedure

Prepared by general procedure III from 4-bromobenzenesulfonyl chloride (5.0 g, 20 mmol) and 2-methoxyethyl amine (1.62 g, 22 mmol) to give the title compound (5.5 g, 95%) as an off-white crystalline solid. MS (ISP) 294.1 [(M+H)+].

Sources & evidence

ORD record
ord-4b90e5cf58814957b562defe8b576de7
Source dataset
uspto-grants-2011_11
Patent number
US08063048B2

Reaction notes

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