HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyethylamine → 3-Bromo-n-(2-methoxyethyl)benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyethylamine | HCID 8018 | — |
| Reactant | m-Bromobenzenesulphonyl chloride | HCID 17943 | — |
| Product | 3-Bromo-n-(2-methoxyethyl)benzenesulfonamide | HCID 47108460 | 99% |
Reaction Steps
Prepared by general procedure III from 3-bromobenzenesulfonyl chloride (5.0 g, 20 mmol) and 2-methoxyethyl amine (1.62 g, 22 mmol) to give the title compound (5.7 g, 99%) as light-yellow liquid. MS (ISP) 294.0 [(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08063048B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-ccec5b52de1b44d28e1757ca3d84a201 |
| Source note | uspto-grants-2011_11 |