2-Methoxyethylamine → 3-Bromo-n-(2-methoxyethyl)benzenesulfonamide

HRID 558516Notes

Reaction equation

[Br:1][C:2]1[CH:3]=[C:4]([S:8](Cl)(=[O:10])=[O:9])[CH:5]=[CH:6][CH:7]=1.[CH3:12][O:13][CH2:14][CH2:15][NH2:16]>>[Br:1][C:2]1[CH:3]=[C:4]([S:8]([NH:16][CH2:15][CH2:14][O:13][CH3:12])(=[O:10])=[O:9])[CH:5]=[CH:6][CH:7]=1

Participants

Reactant 2

HCID 80182-Methoxyethylamine

HCID 17943m-Bromobenzenesulphonyl chloride

Product 1

HCID 471084603-Bromo-n-(2-methoxyethyl)benzenesulfonamideYield 99%

Procedure

Prepared by general procedure III from 3-bromobenzenesulfonyl chloride (5.0 g, 20 mmol) and 2-methoxyethyl amine (1.62 g, 22 mmol) to give the title compound (5.7 g, 99%) as light-yellow liquid. MS (ISP) 294.0 [(M+H)+].

Sources & evidence

ORD record: ord-ccec5b52de1b44d28e1757ca3d84a201
Source dataset: uspto-grants-2011_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08063048B2

Reaction notes

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