反应详情

温度

80 °C

5.5 g of methyl 4-hydrazinobenzoate are dissolved in 38.2 ml of AcOH containing 2.4 g of sodium acetate, and the mixture is heated at 80° C. for 18 hours. The mineral is filter-dried, then evaporation is performed and the product is taken up with a minimum of Et2O. The product is filter-dried so as to obtain 7.97 g of the expected compound.

1. customThe mineral is filter-dried
2. customevaporation
3. customThe product is filter-dried so as