Acetic Acid → Methyl 4-(2-acetylhydrazino)benzoate

Beteiligte Stoffe

Reaktionsbedingungen

Reaktionsschritte

5.5 g of methyl 4-hydrazinobenzoate are dissolved in 38.2 ml of AcOH containing 2.4 g of sodium acetate, and the mixture is heated at 80° C. for 18 hours. The mineral is filter-dried, then evaporation is performed and the product is taken up with a minimum of Et2O. The product is filter-dried so as to obtain 7.97 g of the expected compound.

Herkunft & Nachweise