Hydroxyamine hydrochloride → HCID 66997904, compound

HRID 559151Notes

Reaction equation

HRID 559151 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[C:9]1[C:28](=[O:29])[N:27]([CH3:30])[C:12]2[N:13]([CH3:26])[C:14]3[C:19]([C:11]=2[CH:10]=1)=[CH:18][C:17]([C:20](=[O:25])[CH2:21][C:22](=O)[CH3:23])=[CH:16][CH:15]=3.Cl.[NH2:32]O>>[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[C:9]1[C:28](=[O:29])[N:27]([CH3:30])[C:12]2[N:13]([CH3:26])[C:14]3[C:19]([C:11]=2[CH:10]=1)=[CH:18][C:17]([C:20]1[O:25][N:32]=[C:22]([CH3:23])[CH:21]=1)=[CH:16][CH:15]=3

Participants

3

Reactant 2

HCID 443297Hydroxyamine hydrochlorideHCID 66997466HCID 66997466, compound

Product 1

HCID 66997904HCID 66997904, compound

Procedure

The process is carried out as indicated in Example 44 above, using 1-[3-(2,4-dichlorophenyl)-1,9-dimethyl-2-oxo-2,9-dihydro-1H-pyrido[2,3-b]indol-6-yl]butane-1,3-dione from preparation 1.14 and hydroxylamine hydrochloride.

Sources & evidence

ORD record
ord-970694fe4cba4dfb84e54462d69b9be9
Source dataset
uspto-grants-2011_11
Patent number
US08063061B2

Reaction notes

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