Hydrazine hydrate (1:1) → HCID 66998150, compound

HRID 559169Notes

Reaction equation

HRID 559169 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([O:8][CH3:9])[CH:5]=[CH:4][C:3]=1[C:10]1[C:30](=[O:31])[N:29]([CH3:32])[C:13]2[N:14]([CH3:28])[C:15]3[C:20]([C:12]=2[CH:11]=1)=[CH:19][C:18]([C:21](=O)[CH:22]=[CH:23][N:24](C)C)=[CH:17][CH:16]=3.O.[NH2:34]N>>[Cl:1][C:2]1[CH:7]=[C:6]([O:8][CH3:9])[CH:5]=[CH:4][C:3]=1[C:10]1[C:30](=[O:31])[N:29]([CH3:32])[C:13]2[N:14]([CH3:28])[C:15]3[C:20]([C:12]=2[CH:11]=1)=[CH:19][C:18]([C:21]1[NH:34][N:24]=[CH:23][CH:22]=1)=[CH:17][CH:16]=3

Participants

3

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 66998334HCID 66998334, compound

Product 1

HCID 66998150HCID 66998150, compound

Procedure

The process is carried out as indicated in Example 60 above, using compound D 3-(2-chloro-4-methoxyphenyl)-6-(3-dimethylaminoacryloyl)-1,9-dimethyl-1,9-dihydropyrido[2,3-b]indol-2-one and hydrazine hydrate.

Sources & evidence

ORD record
ord-28d0dae3f0ee440bbaa366779cb7add2
Source dataset
uspto-grants-2011_11
Patent number
US08063061B2

Reaction notes

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