Hydrazine hydrate (1:1) → HCID 66998325, compound

HRID 559232Notes

Reaction equation

HRID 559232 reaction equation
C[N:2](C)[CH:3]=[C:4]([CH3:30])[C:5]([C:7]1[CH:8]=[C:9]2[C:13](=[CH:14][CH:15]=1)[N:12]([CH3:16])[C:11]1[N:17]([CH3:29])[C:18](=[O:28])[C:19]([C:21]3[CH:26]=[CH:25][C:24]([Cl:27])=[CH:23][CH:22]=3)=[CH:20][C:10]2=1)=O.O.[NH2:33]N>>[Cl:27][C:24]1[CH:23]=[CH:22][C:21]([C:19]2[C:18](=[O:28])[N:17]([CH3:29])[C:11]3[N:12]([CH3:16])[C:13]4[C:9]([C:10]=3[CH:20]=2)=[CH:8][C:7]([C:5]2[NH:33][N:2]=[CH:3][C:4]=2[CH3:30])=[CH:15][CH:14]=4)=[CH:26][CH:25]=1

Participants

3

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 66998034HCID 66998034, compound

Product 1

HCID 66998325HCID 66998325, compound

Procedure

The process is carried out as indicated in Example 36 above, with compound B, 6-(3-dimethylamino-2-methyl-acryloyl)-3-(4-chlorophenyl)-1,9-dimethyl-1,9-dihydropyrido[2,3-b]indol-2-one and hydrazine hydrate.

Sources & evidence

ORD record
ord-b434ae3c964e4d76ab72857e21c95a45
Source dataset
uspto-grants-2011_11
Patent number
US08063061B2

Reaction notes

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