HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → HCID 67001472, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | HCID 67001283 | HCID 67001283 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67001472 | HCID 67001472 | — |
Reaction Steps
4-[6-(2,4-Dichloro-phenoxy)-3-oxo-hex-1-enyl]-N-methoxymethyl-N-thiazol-2-yl-benzenesulfonamide (0.259 mmol) and hydrazine (2 mL) was heated to 80° C. in ethanol (15 mL) for 2 h. The solution was concentrated in vacuo. The crude 4-{5-[3-(2,4-dichloro-phenoxy)-propyl]-3,4-dihydro-2H-pyrazol-3-yl}-N-methoxymethyl-N-thiazol-2-yl-benzenesulfonamide was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08063080B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-d44fd7e42c354b669ed50baccc41ba37 |
| Source note | uspto-grants-2011_11 |