HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67001472, compound → HCID 178496786, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67001472 | HCID 67001472 | — |
| Catalyst | Manganese oxide | HCID 160959 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 178496786 | HCID 178496786 | — |
Reaction Steps
A large excess of manganese oxide was added to 4-{5-[3-(2,4-dichloro-phenoxy)-propyl]-3,4-dihydro-2H-pyrazol-3-yl}-N-methoxymethyl-N-thiazol-2-yl-benzenesulfonamide (0.259 mmol) in chloroform (20 mL). After stirring for 4 h the solution was filtered thorough Celite and concentrated in vacuo. The crude 4-{5-[3-(2,4-dichloro-phenoxy)-propyl]-2H-pyrazol-3-yl}-N-methoxymethyl-N-thiazol-2-yl-benzenesulfonamide was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08063080B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-a09dff9b8d844f6daf6e10ad4e55990c |
| Source note | uspto-grants-2011_11 |