HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67001255, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 44549018 | HCID 44549018 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67001255 | HCID 67001255 | — |
Reaction Steps
3-(3′-methanesulfonyl-biphenyl-3-yl)-4-o-tolyl-piperazine-1-carboxylic acid tert-butyl ester (90 mg) in ethanol (1 mL) was treated with a saturated solution of HCl in ethanol (1 mL) at room temperature overnight. The solution was concentrated in vacuo to yield crude 2-(3′-methanesulfonyl-biphenyl-3-yl)-1-o-tolyl-piperazine hydrochloride, MS: 407.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08063088B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-73ab7cabd5ae48fdb3aef616ad88bcc0 |
| Source note | uspto-grants-2011_11 |